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Beilstein J. Org. Chem. 2009, 5, No. 30, doi:10.3762/bjoc.5.30
Graphical Abstract
Scheme 1: Azide addition to aldehydes and formation of carbamoyl azides.
Figure 1: Microreactor setup for the in situ generation and use of iodine azide (IN3).
Scheme 2: Reaction of carbamoyl azide 4a with n-butyllithium.